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Détail de l'indexation
D003682
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Ouvrages de la bibliothèque en indexation D003682
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Synthèses d'acides aminés N-acyles par amido-carbonylation d'aldéhydes / Dominique Reffet
Titre : Synthèses d'acides aminés N-acyles par amido-carbonylation d'aldéhydes : extensions à d'autres substrats Type de document : texte imprimé Auteurs : Dominique Reffet, Auteur ; F. Petit, Directeur de thèse Editeur : Université de Paris-Sud Année de publication : 1982 Importance : 129 f. Présentation : ill. Format : 27 cm. Note générale : Thèse de Docteur Ingénieur : Chimie organique : Pris, Université de Paris-Sud : 1982
Bibliogr. f. 130 . Annexe f. 131 - 133Langues : Français (fre) Mots-clés : Aldéhydes
Réactions -- glycination
Glycination -- oléfines
Réaction -- amido-carbonylation
Acides -- aminés N-acylesIndex. décimale : D003682 Résumé : Parmi les réactions de carbonylation, une des plus anciennes est l'hydroformylation ou réaction "oxo" découverte par Roelen en 1938.
Cette réaction consiste à additionner l'oxyde de carbone et l'hydrogène sur une double liaison oléfinique en présence d'un catalyseur homogène, pour former un composé comportant un carbone.
Le champ d'applications envisagé pour ces produits, met en évidence la nécessité de trouver une synthèse économique basée sur des intermédiaires accessibles.
Dans un premier temps, nous nous sommes intéressés à la réaction d'amido-carbonylation des aldéhydes, pour en déterminer quelques caractères généraux.
Cette étude, en plus des traits principaux nous a permis de mettre en évidence une réactivité particulière du formol.
Puis, en nous basant sur la similitude de conditions opératoires avec la réaction oxo, nous avons envisagé de réaliser la glycination d'oléfines et d'en étudier certains paramètres.
Cette réaction, qui réalise simultanément l'hydroformylation et l'amido-carbonylation, a donné des résultats tout à fait positifs.
Enfin, nous avons essayé d'associer, dans le même esprit, l'amido-carbonylation à d'autres réactions de carbonylation plusclassiques.Synthèses d'acides aminés N-acyles par amido-carbonylation d'aldéhydes : extensions à d'autres substrats [texte imprimé] / Dominique Reffet, Auteur ; F. Petit, Directeur de thèse . - [S.l.] : Université de Paris-Sud, 1982 . - 129 f. : ill. ; 27 cm.
Thèse de Docteur Ingénieur : Chimie organique : Pris, Université de Paris-Sud : 1982
Bibliogr. f. 130 . Annexe f. 131 - 133
Langues : Français (fre)
Mots-clés : Aldéhydes
Réactions -- glycination
Glycination -- oléfines
Réaction -- amido-carbonylation
Acides -- aminés N-acylesIndex. décimale : D003682 Résumé : Parmi les réactions de carbonylation, une des plus anciennes est l'hydroformylation ou réaction "oxo" découverte par Roelen en 1938.
Cette réaction consiste à additionner l'oxyde de carbone et l'hydrogène sur une double liaison oléfinique en présence d'un catalyseur homogène, pour former un composé comportant un carbone.
Le champ d'applications envisagé pour ces produits, met en évidence la nécessité de trouver une synthèse économique basée sur des intermédiaires accessibles.
Dans un premier temps, nous nous sommes intéressés à la réaction d'amido-carbonylation des aldéhydes, pour en déterminer quelques caractères généraux.
Cette étude, en plus des traits principaux nous a permis de mettre en évidence une réactivité particulière du formol.
Puis, en nous basant sur la similitude de conditions opératoires avec la réaction oxo, nous avons envisagé de réaliser la glycination d'oléfines et d'en étudier certains paramètres.
Cette réaction, qui réalise simultanément l'hydroformylation et l'amido-carbonylation, a donné des résultats tout à fait positifs.
Enfin, nous avons essayé d'associer, dans le même esprit, l'amido-carbonylation à d'autres réactions de carbonylation plusclassiques.Exemplaires
Code-barres Cote Support Localisation Section Disponibilité Spécialité Etat_Exemplaire D003682 D003682 Papier Bibliothèque centrale Thèse de Doctorat Disponible