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Structural and optical properties of encapsulated ZnO in porous host matrix / Noppadon Sathitsuksanoh in Acta materialia, Vol. 58 N° 2 (Janvier 2010) 

Public ISBD [article]  in Acta materialia > Vol. 58 N° 2 (Janvier 2010) . - pp. 373-378 Titre : Structural and optical properties of encapsulated ZnO in porous host matrix Type de document : texte imprimé Auteurs : Noppadon Sathitsuksanoh, Auteur ; Dake Wang, Auteur ; HongYun Yang, Auteur Article en page(s) : pp. 373-378 Note générale : Métallurgie Langues : Anglais (eng) Mots-clés : ZnO  Nanoparticles  Impregnation  Raman  Photoluminescence Index. décimale : 669 Métallurgie Résumé : ZnO nanoparticles were encapsulated in the porous activated carbon matrix by incipient-wetness impregnation. The use of the small host matrix allowed the size confinement of ZnO by utilizing the porous nature of the host matrix. Partial fixation of ZnO in the porous matrix determines the size and the dispersion of the particles. Experiments at different calcination temperatures were carried out to investigate structural and optical properties of ZnO nanoparticles in the porous activated carbon matrix using X-ray diffraction, scanning electron microscopy, Raman spectroscopy and photoluminescence. The optimal calcination temperature was found to be not, vert, similar450 °C in order to confine ZnO nanoparticles in the porous ACP matrix. Near-band-edge UV emission and green emission were both associated with the deep-level defect state. A decrease in full width at half maximum of E2 mode in Raman spectrum confirmed an increase in crystallite size due to higher calcination temperature, causing an increase in phonon lifetime. DEWEY : 669 ISSN : 1359-6454 En ligne : http://www.sciencedirect.com/science?_ob=PublicationURL&_tockey=%23TOC%235556%23 [...] [article] Structural and optical properties of encapsulated ZnO in porous host matrix [texte imprimé] / Noppadon Sathitsuksanoh, Auteur ; Dake Wang, Auteur ; HongYun Yang, Auteur . - pp. 373-378. Métallurgie Langues : Anglais (eng) in Acta materialia > Vol. 58 N° 2 (Janvier 2010) . - pp. 373-378 Mots-clés : ZnO  Nanoparticles  Impregnation  Raman  Photoluminescence Index. décimale : 669 Métallurgie Résumé : ZnO nanoparticles were encapsulated in the porous activated carbon matrix by incipient-wetness impregnation. The use of the small host matrix allowed the size confinement of ZnO by utilizing the porous nature of the host matrix. Partial fixation of ZnO in the porous matrix determines the size and the dispersion of the particles. Experiments at different calcination temperatures were carried out to investigate structural and optical properties of ZnO nanoparticles in the porous activated carbon matrix using X-ray diffraction, scanning electron microscopy, Raman spectroscopy and photoluminescence. The optimal calcination temperature was found to be not, vert, similar450 °C in order to confine ZnO nanoparticles in the porous ACP matrix. Near-band-edge UV emission and green emission were both associated with the deep-level defect state. A decrease in full width at half maximum of E2 mode in Raman spectrum confirmed an increase in crystallite size due to higher calcination temperature, causing an increase in phonon lifetime. DEWEY : 669 ISSN : 1359-6454 En ligne : http://www.sciencedirect.com/science?_ob=PublicationURL&_tockey=%23TOC%235556%23 [...]