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Effect of preparation method on the anti-corrosive properties of nanocrystalline Zn–CoO ceramic pigments / S. Rasouli in Materials and corrosion, Vol. 62 N° 5 (Mai 2011) 

Public ISBD [article]  in Materials and corrosion > Vol. 62 N° 5 (Mai 2011) . - pp. 405–410 Titre : Effect of preparation method on the anti-corrosive properties of nanocrystalline Zn–CoO ceramic pigments Type de document : texte imprimé Auteurs : S. Rasouli, Auteur ; I. Danaee, Auteur Année de publication : 2011 Article en page(s) : pp. 405–410 Note générale : Génie Mécanique Langues : Anglais (eng) Mots-clés : Anti-corrosive  High  energy  milling  Mild  steel  electrode  Pigment  Solution  combustion Index. décimale : 620.1 Essais des matériaux. Défauts des matériaux. Protection des matériaux Résumé : Zn–CoO green ceramic pigments were synthesized by two different methods; high energy ball milling and solution combustion, with two different fuels; citric acid and glycine. Products were characterized by X-ray diffraction and scanning–transmission electron microscopy (TEM). The anti-corrosive properties of the obtained pigments were investigated by electrochemical impedance spectroscopy (EIS) techniques. Results have shown that either by solid state reaction or combustion by citric acid, a calcination step was needed to obtain the desired phase whereas by glycine fuel, pure ZnO phase was obtained directly. TEM showed particles with mean particle size of about 70, 150, and 180 nm for glycine, citric acid, and solid state reaction samples, respectively. The corrosion performance of the coating in 3% w/v NaCl solution was evaluated by EIS and polarization measurements. According to the measurements of EIS and electrochemical polarization, the coatings with glycine-based pigment showed the highest corrosion resistance among the prepared coatings. DEWEY : 620.1 ISSN : 0947-5117 En ligne : http://onlinelibrary.wiley.com/doi/10.1002/maco.201005758/abstract [article] Effect of preparation method on the anti-corrosive properties of nanocrystalline Zn–CoO ceramic pigments [texte imprimé] / S. Rasouli, Auteur ; I. Danaee, Auteur . - 2011 . - pp. 405–410. Génie Mécanique Langues : Anglais (eng) in Materials and corrosion > Vol. 62 N° 5 (Mai 2011) . - pp. 405–410 Mots-clés : Anti-corrosive  High  energy  milling  Mild  steel  electrode  Pigment  Solution  combustion Index. décimale : 620.1 Essais des matériaux. Défauts des matériaux. Protection des matériaux Résumé : Zn–CoO green ceramic pigments were synthesized by two different methods; high energy ball milling and solution combustion, with two different fuels; citric acid and glycine. Products were characterized by X-ray diffraction and scanning–transmission electron microscopy (TEM). The anti-corrosive properties of the obtained pigments were investigated by electrochemical impedance spectroscopy (EIS) techniques. Results have shown that either by solid state reaction or combustion by citric acid, a calcination step was needed to obtain the desired phase whereas by glycine fuel, pure ZnO phase was obtained directly. TEM showed particles with mean particle size of about 70, 150, and 180 nm for glycine, citric acid, and solid state reaction samples, respectively. The corrosion performance of the coating in 3% w/v NaCl solution was evaluated by EIS and polarization measurements. According to the measurements of EIS and electrochemical polarization, the coatings with glycine-based pigment showed the highest corrosion resistance among the prepared coatings. DEWEY : 620.1 ISSN : 0947-5117 En ligne : http://onlinelibrary.wiley.com/doi/10.1002/maco.201005758/abstract