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Optimization of carbonization process for preparation of high performance hollow fiber carbon membranes / Xuezhong He in Industrial & engineering chemistry research, Vol. 50 N° 13 (Juillet 2011) 

Public ISBD [article]  in Industrial & engineering chemistry research > Vol. 50 N° 13 (Juillet 2011) . - pp. 8065-8072 Titre : Optimization of carbonization process for preparation of high performance hollow fiber carbon membranes Type de document : texte imprimé Auteurs : Xuezhong He, Auteur ; May - Britt Hagg, Auteur Année de publication : 2011 Article en page(s) : pp. 8065-8072 Note générale : Chimie industrielle Langues : Anglais (eng) Mots-clés : Inorganic  membrane  Hollow  fiber  Preparation  Carbonization  Optimization Résumé : Orthogonal experimental design (OED) was employed to study the influences of carbonization process on the transport properties of hollow fiber carbon membranes (HFCMs). The conjoint analysis method was applied for the statistical analysis of OED results, and the importance of the investigated carbonization parameters on the performance of carbon membrane was found to be: purge gas > final carbonization temperature > heating rate > final soak time. A high performance hollow fiber carbon membrane (HFCM-5) was prepared from the optimal carbonization process. The carbon membrane structure and morphology were characterized by a Fourier transform infrared spectroscopy and a scanning electron microscope. The influences of the operating parameters such as temperature, pressure, and stage-cut on the carbon membrane performances were investigated by the single gas and gas mixture tests. DEWEY : 660 ISSN : 0888-5885 En ligne : http://cat.inist.fr/?aModele=afficheN&cpsidt=24332132 [article] Optimization of carbonization process for preparation of high performance hollow fiber carbon membranes [texte imprimé] / Xuezhong He, Auteur ; May - Britt Hagg, Auteur . - 2011 . - pp. 8065-8072. Chimie industrielle Langues : Anglais (eng) in Industrial & engineering chemistry research > Vol. 50 N° 13 (Juillet 2011) . - pp. 8065-8072 Mots-clés : Inorganic  membrane  Hollow  fiber  Preparation  Carbonization  Optimization Résumé : Orthogonal experimental design (OED) was employed to study the influences of carbonization process on the transport properties of hollow fiber carbon membranes (HFCMs). The conjoint analysis method was applied for the statistical analysis of OED results, and the importance of the investigated carbonization parameters on the performance of carbon membrane was found to be: purge gas > final carbonization temperature > heating rate > final soak time. A high performance hollow fiber carbon membrane (HFCM-5) was prepared from the optimal carbonization process. The carbon membrane structure and morphology were characterized by a Fourier transform infrared spectroscopy and a scanning electron microscope. The influences of the operating parameters such as temperature, pressure, and stage-cut on the carbon membrane performances were investigated by the single gas and gas mixture tests. DEWEY : 660 ISSN : 0888-5885 En ligne : http://cat.inist.fr/?aModele=afficheN&cpsidt=24332132