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Improved performance of poly(Vinylidene Fluoride) microfiltration membranes prepared by freeze and immersion precipitation coupling method / Su, Yanlei in Industrial & engineering chemistry research, Vol. 50 N° 18 (Septembre 2011) 

Public ISBD [article]  in Industrial & engineering chemistry research > Vol. 50 N° 18 (Septembre 2011) . - pp. 10525-10532 Titre : Improved performance of poly(Vinylidene Fluoride) microfiltration membranes prepared by freeze and immersion precipitation coupling method Type de document : texte imprimé Auteurs : Su, Yanlei, Auteur ; Yangui Liang, Auteur ; Chunxia Mu, Auteur Année de publication : 2011 Article en page(s) : pp. 10525-10532 Note générale : Chimie industrielle Langues : Anglais (eng) Mots-clés : Immersion  Membrane  separation  Microfiltration Résumé : Cellulose acetate (CA) was used as a hydrophilic additive to blend with poly(vinylidene fluoride) (PVDF) for preparing casting solutions. A novel freeze and immersion precipitation coupling method was developed to improve the performance of PVDF microporous membranes. X-ray photoelectron spectroscopy (XPS) analysis confirmed the enrichment of CA segments on the PVDF membrane surfaces. The level of CA surface segregation on PVDF membrane surfaces was dramatically influenced by the freezing time. The hypothesis ofsolid (frozen DMSO)—liquid—solid (precipitated polymer) phase separation was proposed to explain the CA surface enrichment phenomenon. The mechanical strength and antifouling property of the PVDF microfiltration membranes were simultaneously improved by the synergistic action of freeze and immersion precipitation coupling technique. The PVDF microfiltration membranes exhibited higher permeability and better antifouling property in bioseparation process than that fabricated by the individual freeze technique. DEWEY : 660 ISSN : 0888-5885 En ligne : http://cat.inist.fr/?aModele=afficheN&cpsidt=24523875 [article] Improved performance of poly(Vinylidene Fluoride) microfiltration membranes prepared by freeze and immersion precipitation coupling method [texte imprimé] / Su, Yanlei, Auteur ; Yangui Liang, Auteur ; Chunxia Mu, Auteur . - 2011 . - pp. 10525-10532. Chimie industrielle Langues : Anglais (eng) in Industrial & engineering chemistry research > Vol. 50 N° 18 (Septembre 2011) . - pp. 10525-10532 Mots-clés : Immersion  Membrane  separation  Microfiltration Résumé : Cellulose acetate (CA) was used as a hydrophilic additive to blend with poly(vinylidene fluoride) (PVDF) for preparing casting solutions. A novel freeze and immersion precipitation coupling method was developed to improve the performance of PVDF microporous membranes. X-ray photoelectron spectroscopy (XPS) analysis confirmed the enrichment of CA segments on the PVDF membrane surfaces. The level of CA surface segregation on PVDF membrane surfaces was dramatically influenced by the freezing time. The hypothesis ofsolid (frozen DMSO)—liquid—solid (precipitated polymer) phase separation was proposed to explain the CA surface enrichment phenomenon. The mechanical strength and antifouling property of the PVDF microfiltration membranes were simultaneously improved by the synergistic action of freeze and immersion precipitation coupling technique. The PVDF microfiltration membranes exhibited higher permeability and better antifouling property in bioseparation process than that fabricated by the individual freeze technique. DEWEY : 660 ISSN : 0888-5885 En ligne : http://cat.inist.fr/?aModele=afficheN&cpsidt=24523875