A gel sample preparation method for the analysis of zinc concentrates by WD-XRF / Gai Zhang in Minerals engineering, Vol. 22 N° 4 (Mars 2009)  

Public ISBD [article]  inMinerals engineering > Vol. 22 N° 4 (Mars 2009) . - pp. 348–351 Titre : A gel sample preparation method for the analysis of zinc concentrates by WD-XRF Type de document : texte imprimé Auteurs : Gai Zhang, Auteur ; Xudong Hu, Auteur ; Hairui Ma, Auteur Année de publication : 2009 Article en page(s) : pp. 348–351 Note générale : Génie Minier Langues : Anglais (eng) Mots-clés : X-ray fluorescence Gel Sample preparation Zinc concentrates Résumé : This article describes a methodology for analyzing zinc in zinc concentrates materials by wavelength-dispersive X-ray fluorescence (WD-XRF) spectrometry with gel for sample preparation. The sample was decomposed with aqua regia. The sample solution mixed with agaron gel was heated to boiling. The mixture became quasi-solid gel under normal temperature. The elements dispersed in gel medium were detected by WD-XRF spectrometry. The method has both advantages of the solution preparation method and the solid preparation method. In addition, this method was adapted in detecting high content ores, because it avoided the risking of using platinum crucible. The method has been applied to the determination of lead, zinc and iron in zinc concentrates successfully. DEWEY : 622 ISSN : 0892-6875 En ligne : http://www.sciencedirect.com/science/article/pii/S0892687508002392 [article] A gel sample preparation method for the analysis of zinc concentrates by WD-XRF [texte imprimé] / Gai Zhang, Auteur ; Xudong Hu, Auteur ; Hairui Ma, Auteur . - 2009 . - pp. 348–351. Génie Minier Langues : Anglais (eng) in Minerals engineering > Vol. 22 N° 4 (Mars 2009) . - pp. 348–351 Mots-clés : X-ray fluorescence Gel Sample preparation Zinc concentrates Résumé : This article describes a methodology for analyzing zinc in zinc concentrates materials by wavelength-dispersive X-ray fluorescence (WD-XRF) spectrometry with gel for sample preparation. The sample was decomposed with aqua regia. The sample solution mixed with agaron gel was heated to boiling. The mixture became quasi-solid gel under normal temperature. The elements dispersed in gel medium were detected by WD-XRF spectrometry. The method has both advantages of the solution preparation method and the solid preparation method. In addition, this method was adapted in detecting high content ores, because it avoided the risking of using platinum crucible. The method has been applied to the determination of lead, zinc and iron in zinc concentrates successfully. DEWEY : 622 ISSN : 0892-6875 En ligne : http://www.sciencedirect.com/science/article/pii/S0892687508002392

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