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Evaluation of leaching parameters for a refractory gold ore containing aurostibite and antimony minerals / G. Deschênes in Minerals engineering, Vol. 22 N° 9/10 (Août/Septembre 2009) 

Public ISBD [article]  in Minerals engineering > Vol. 22 N° 9/10 (Août/Septembre 2009) . - pp. 799–808 Titre : Evaluation of leaching parameters for a refractory gold ore containing aurostibite and antimony minerals : Part I – Central zone Type de document : texte imprimé Auteurs : G. Deschênes, Auteur ; C. Xia, Auteur ; M. Fulton, Auteur Année de publication : 2009 Article en page(s) : pp. 799–808 Note générale : Génie Minier Langues : Anglais (eng) Mots-clés : Gold  Aurostibite  Stibnite  Lead  nitrate  Sulphide  Freewest  Cyanide  Hydroseparation Résumé : A cyanidation study was conducted on a mild refractory gold ore sample from the Central zone of Clarence Stream Property, owned by Freewest Resources Canada, to develop a leaching strategy to extract gold. Gold, at a grade of 8.00 g/t, is present as native gold, electrum and aurostibite. The ore also contains 2.8% pyrrhotite, together with several antimony minerals (0.8% berthierite and gudmundite, 0.18% native antimony and stibnite). It also exhibits weak preg-robbing properties with 0.16% organic carbon. Aurostibite, a gold antimony compound, is particularly known to be insoluble in cyanide solution. The antimony dissolves in cyanide solution to form antimonates, which retards gold dissolution. Industrial practice of extracting gold from aurostibite generally consists of producing a flotation concentrate, which is leached in a pipe reactor at low alkalinity and high oxygen pressure with about 20 g/L cyanide. The proposed new approach is efficient and allows the extraction of gold directly from an ore at atmospheric pressure and a low cyanide concentration at pH 10.5. The effects of grinding, pre-treatment, lead nitrate, kerosene and cyanide concentrations have been investigated. The maximum gold extraction obtained on the ore was 87.9% using 800 ppm NaCN, 500 g/t lead nitrate, 30 g/t kerosene, DO (dissolved oxygen) 10 ppm and pH 10.5 in 168 h. The associated cyanide consumption was 1.3 kg/t. The additions of lead nitrate and kerosene increased gold extraction. In comparison to a P80 of 74 μm, a P80 of 30 μm significantly increased gold extraction. Gold in solid solution in gudmundite and arsenopyrite was believed to be responsible for the un-leached fraction until mineralogical analysis of hydroseparation concentrates of leach residues showed that most of the un-leached gold occurs as aurostibite, either as locked grains in sulphides/sulpharsenides or as grains with passivation rims of an Au–Sb–O phase. Coarse gold was also found. Gold extraction was not sensitive to cyanide concentration from 250 to 1200 ppm NaCN and high pH was detrimental. Decreasing the cyanide concentration reduced the cyanide consumption from 1.39 to 0.85 kg/t. The removal of coarse gold using a Knelson concentrator and a Mosley table prior to leaching increased the gold extraction to 90.4% (leach residue at 0.77 g/t). DEWEY : 622 ISSN : 0892-6875 En ligne : http://www.sciencedirect.com/science/article/pii/S0892687509000508 [article] Evaluation of leaching parameters for a refractory gold ore containing aurostibite and antimony minerals : Part I – Central zone [texte imprimé] / G. Deschênes, Auteur ; C. Xia, Auteur ; M. Fulton, Auteur . - 2009 . - pp. 799–808. Génie Minier Langues : Anglais (eng) in Minerals engineering > Vol. 22 N° 9/10 (Août/Septembre 2009) . - pp. 799–808 Mots-clés : Gold  Aurostibite  Stibnite  Lead  nitrate  Sulphide  Freewest  Cyanide  Hydroseparation Résumé : A cyanidation study was conducted on a mild refractory gold ore sample from the Central zone of Clarence Stream Property, owned by Freewest Resources Canada, to develop a leaching strategy to extract gold. Gold, at a grade of 8.00 g/t, is present as native gold, electrum and aurostibite. The ore also contains 2.8% pyrrhotite, together with several antimony minerals (0.8% berthierite and gudmundite, 0.18% native antimony and stibnite). It also exhibits weak preg-robbing properties with 0.16% organic carbon. Aurostibite, a gold antimony compound, is particularly known to be insoluble in cyanide solution. The antimony dissolves in cyanide solution to form antimonates, which retards gold dissolution. Industrial practice of extracting gold from aurostibite generally consists of producing a flotation concentrate, which is leached in a pipe reactor at low alkalinity and high oxygen pressure with about 20 g/L cyanide. The proposed new approach is efficient and allows the extraction of gold directly from an ore at atmospheric pressure and a low cyanide concentration at pH 10.5. The effects of grinding, pre-treatment, lead nitrate, kerosene and cyanide concentrations have been investigated. The maximum gold extraction obtained on the ore was 87.9% using 800 ppm NaCN, 500 g/t lead nitrate, 30 g/t kerosene, DO (dissolved oxygen) 10 ppm and pH 10.5 in 168 h. The associated cyanide consumption was 1.3 kg/t. The additions of lead nitrate and kerosene increased gold extraction. In comparison to a P80 of 74 μm, a P80 of 30 μm significantly increased gold extraction. Gold in solid solution in gudmundite and arsenopyrite was believed to be responsible for the un-leached fraction until mineralogical analysis of hydroseparation concentrates of leach residues showed that most of the un-leached gold occurs as aurostibite, either as locked grains in sulphides/sulpharsenides or as grains with passivation rims of an Au–Sb–O phase. Coarse gold was also found. Gold extraction was not sensitive to cyanide concentration from 250 to 1200 ppm NaCN and high pH was detrimental. Decreasing the cyanide concentration reduced the cyanide consumption from 1.39 to 0.85 kg/t. The removal of coarse gold using a Knelson concentrator and a Mosley table prior to leaching increased the gold extraction to 90.4% (leach residue at 0.77 g/t). DEWEY : 622 ISSN : 0892-6875 En ligne : http://www.sciencedirect.com/science/article/pii/S0892687509000508