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n - Propyl propionate synthesis via catalytic distillation - experimental investigation in pilot - scale / Carsten Buchaly in Industrial & engineering chemistry research, Vol. 51 N° 2 (Janvier 2012) 

Public ISBD [article]  in Industrial & engineering chemistry research > Vol. 51 N° 2 (Janvier 2012) . - pp. 891-899 Titre : n - Propyl propionate synthesis via catalytic distillation - experimental investigation in pilot - scale Type de document : texte imprimé Auteurs : Carsten Buchaly, Auteur ; Peter Kreis, Auteur Année de publication : 2012 Article en page(s) : pp. 891-899 Note générale : Chimie industrielle Langues : Anglais (eng) Mots-clés : Distillation  Catalytic  reaction Résumé : Catalytic distillation experiments were designed and carried out in a pilot-scale column to prove the technical feasibility of the heterogeneously catalyzed n-propyl propionate synthesis by esterification of propionic acid with 1-propanol using the surface-sulfonated ion-exchange resin Amberlyst 46. The experiments cover a broad range of decisive operational parameters, for example, reflux ratio, column load, distillate-to-feed ratio, and molar feed ratio of the reactants. The reconciled results comprise a complete set of concentration and temperature profiles along the column height and, hence, exhibit detailed and reliable data for model validation purposes. DEWEY : 660 ISSN : 0888-5885 En ligne : http://cat.inist.fr/?aModele=afficheN&cpsidt=25476422 [article] n - Propyl propionate synthesis via catalytic distillation - experimental investigation in pilot - scale [texte imprimé] / Carsten Buchaly, Auteur ; Peter Kreis, Auteur . - 2012 . - pp. 891-899. Chimie industrielle Langues : Anglais (eng) in Industrial & engineering chemistry research > Vol. 51 N° 2 (Janvier 2012) . - pp. 891-899 Mots-clés : Distillation  Catalytic  reaction Résumé : Catalytic distillation experiments were designed and carried out in a pilot-scale column to prove the technical feasibility of the heterogeneously catalyzed n-propyl propionate synthesis by esterification of propionic acid with 1-propanol using the surface-sulfonated ion-exchange resin Amberlyst 46. The experiments cover a broad range of decisive operational parameters, for example, reflux ratio, column load, distillate-to-feed ratio, and molar feed ratio of the reactants. The reconciled results comprise a complete set of concentration and temperature profiles along the column height and, hence, exhibit detailed and reliable data for model validation purposes. DEWEY : 660 ISSN : 0888-5885 En ligne : http://cat.inist.fr/?aModele=afficheN&cpsidt=25476422