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Core–shell nanoscale precipitates in Al–0.06 at.% Sc microalloyed with Tb, Ho, Tm or Lu / Matthew E. Krug in Acta materialia, Vol. 58 N° 1 (Janvier 2010) 

Public ISBD [article]  in Acta materialia > Vol. 58 N° 1 (Janvier 2010) . - pp. 134–145 Titre : Core–shell nanoscale precipitates in Al–0.06 at.% Sc microalloyed with Tb, Ho, Tm or Lu Type de document : texte imprimé Auteurs : Matthew E. Krug, Auteur ; Alexandra Werber, Auteur ; David C. Dunand, Auteur Année de publication : 2010 Article en page(s) : pp. 134–145 Note générale : Métallurgie Langues : Anglais (eng) Mots-clés : Rare  earth  Precipitation  Microhardness  Atom-probe  field-ion  microscopy  (AP-FIM)  Aluminum  alloys Résumé : The age-hardening response at 300 °C of Al–0.06Sc–0.02RE (at.%, with RE = Tb, Ho, Tm or Lu) is found to be similar to that of binary Al–0.08Sc (at.%), except that a shorter incubation period for hardening is observed, which is associated with nanoscale RE-rich Al3(RE1−xScx) precipitates. In addition, Al–0.06Sc–0.02Tb (at.%) has a much lower peak microhardness than that of Al–0.08Sc (at.%) due to the small solubility of Tb in α-Al(Sc). Peak-age hardening occurs after 24 h, and is associated with a high number density of nanoscale Sc-rich Al3(Sc1−xREx) precipitates. Analysis by three-dimensional local-electrode atom-probe tomography shows that x increases with increasing atomic number, and that the REs partition to the core of the precipitates. DEWEY : 669 ISSN : 1359-6454 En ligne : http://www.sciencedirect.com/science/article/pii/S1359645409005874 [article] Core–shell nanoscale precipitates in Al–0.06 at.% Sc microalloyed with Tb, Ho, Tm or Lu [texte imprimé] / Matthew E. Krug, Auteur ; Alexandra Werber, Auteur ; David C. Dunand, Auteur . - 2010 . - pp. 134–145. Métallurgie Langues : Anglais (eng) in Acta materialia > Vol. 58 N° 1 (Janvier 2010) . - pp. 134–145 Mots-clés : Rare  earth  Precipitation  Microhardness  Atom-probe  field-ion  microscopy  (AP-FIM)  Aluminum  alloys Résumé : The age-hardening response at 300 °C of Al–0.06Sc–0.02RE (at.%, with RE = Tb, Ho, Tm or Lu) is found to be similar to that of binary Al–0.08Sc (at.%), except that a shorter incubation period for hardening is observed, which is associated with nanoscale RE-rich Al3(RE1−xScx) precipitates. In addition, Al–0.06Sc–0.02Tb (at.%) has a much lower peak microhardness than that of Al–0.08Sc (at.%) due to the small solubility of Tb in α-Al(Sc). Peak-age hardening occurs after 24 h, and is associated with a high number density of nanoscale Sc-rich Al3(Sc1−xREx) precipitates. Analysis by three-dimensional local-electrode atom-probe tomography shows that x increases with increasing atomic number, and that the REs partition to the core of the precipitates. DEWEY : 669 ISSN : 1359-6454 En ligne : http://www.sciencedirect.com/science/article/pii/S1359645409005874