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Towards smooth and pure iron nanowires grown by electrodeposition in self-organized alumina membranes / V. Haehnel in Acta materialia, Vol. 58 N° 7 (Avril 2010) 

Public ISBD [article]  in Acta materialia > Vol. 58 N° 7 (Avril 2010) . - pp. 2330–2337 Titre : Towards smooth and pure iron nanowires grown by electrodeposition in self-organized alumina membranes Type de document : texte imprimé Auteurs : V. Haehnel, Auteur ; S. Fähler, Auteur ; P. Schaaf, Auteur Année de publication : 2011 Article en page(s) : pp. 2330–2337 Note générale : Métallurgie Langues : Anglais (eng) Mots-clés : Electrodeposition  AAO  template  Iron  nanowires  Mössbauer  spectroscopy Résumé : Due to their high aspect ratio, magnetic nanowires are interesting for various applications. Fe nanowires are of particular interest due to their high magnetization, which suggests high shape anisotropy is possible. Here, we show how the electrodeposition process can be adapted to the constraints of a high aspect ratio template in order to approach an ideal behaviour of smooth and pure Fe nanowires. An adjustment of the Fe2+ concentration and the addition of H3BO3 result in smooth and continuous nanowires; saturation polarization is achieved, together with an anisotropy field of up to 70% compared to pure Fe. Mössbauer spectroscopy reveals a negligible amount of impurities. Together with magnetic measurements we show that shape anisotropy aligns the preferential magnetization axis along the wire axis. DEWEY : 669 ISSN : 1359-6454 En ligne : http://www.sciencedirect.com/science/article/pii/S1359645409008611 [article] Towards smooth and pure iron nanowires grown by electrodeposition in self-organized alumina membranes [texte imprimé] / V. Haehnel, Auteur ; S. Fähler, Auteur ; P. Schaaf, Auteur . - 2011 . - pp. 2330–2337. Métallurgie Langues : Anglais (eng) in Acta materialia > Vol. 58 N° 7 (Avril 2010) . - pp. 2330–2337 Mots-clés : Electrodeposition  AAO  template  Iron  nanowires  Mössbauer  spectroscopy Résumé : Due to their high aspect ratio, magnetic nanowires are interesting for various applications. Fe nanowires are of particular interest due to their high magnetization, which suggests high shape anisotropy is possible. Here, we show how the electrodeposition process can be adapted to the constraints of a high aspect ratio template in order to approach an ideal behaviour of smooth and pure Fe nanowires. An adjustment of the Fe2+ concentration and the addition of H3BO3 result in smooth and continuous nanowires; saturation polarization is achieved, together with an anisotropy field of up to 70% compared to pure Fe. Mössbauer spectroscopy reveals a negligible amount of impurities. Together with magnetic measurements we show that shape anisotropy aligns the preferential magnetization axis along the wire axis. DEWEY : 669 ISSN : 1359-6454 En ligne : http://www.sciencedirect.com/science/article/pii/S1359645409008611