Three-dimensional analysis of microstructures in titanium / Hemant Sharma in Acta materialia, Vol. 58 N° 7 (Avril 2010)  

Public ISBD [article]  inActa materialia > Vol. 58 N° 7 (Avril 2010) . - pp. 2399–2407 Titre : Three-dimensional analysis of microstructures in titanium Type de document : texte imprimé Auteurs : Hemant Sharma, Auteur ; Stefan M.C. Van Bohemen, Auteur ; Roumen H. Petrov, Auteur Année de publication : 2011 Article en page(s) : pp. 2399–2407 Note générale : Métallurgie Langues : Anglais (eng) Mots-clés : EBSD Titanium alloys Grain morphology Serial sectioning Résumé : Samples of Ti–4.3Fe–6.7Mo–1.5Al were isothermally annealed in the temperature range of 730–780 °C for various times to study the β–α transformation. Serial sectioning in conjunction with both optical and EBSD analyses was applied to determine the three-dimensional (3-D) morphologies of primary α phase. The 3-D analysis proved to be essential for characterization of the complex morphologies of α grains and consequently for the identification of growth behavior. It showed that nucleation of α grains takes place at β–β grain boundaries and significant branching takes place after initial growth of α grains along β–β grain boundaries. Some branches grow inside the β grain interior. The branching behavior is shown to interact with β–β grain boundaries, leading to a zig-zag morphology. The presented 3-D analysis of α grains and their influence on β–β grain boundaries clearly show that 2-D observations of the microstructural morphologies are not sufficient to adequately represent the transformation characteristics. DEWEY : 669 ISSN : 1359-6454 En ligne : http://www.sciencedirect.com/science/article/pii/S1359645409008726 [article] Three-dimensional analysis of microstructures in titanium [texte imprimé] / Hemant Sharma, Auteur ; Stefan M.C. Van Bohemen, Auteur ; Roumen H. Petrov, Auteur . - 2011 . - pp. 2399–2407. Métallurgie Langues : Anglais (eng) in Acta materialia > Vol. 58 N° 7 (Avril 2010) . - pp. 2399–2407 Mots-clés : EBSD Titanium alloys Grain morphology Serial sectioning Résumé : Samples of Ti–4.3Fe–6.7Mo–1.5Al were isothermally annealed in the temperature range of 730–780 °C for various times to study the β–α transformation. Serial sectioning in conjunction with both optical and EBSD analyses was applied to determine the three-dimensional (3-D) morphologies of primary α phase. The 3-D analysis proved to be essential for characterization of the complex morphologies of α grains and consequently for the identification of growth behavior. It showed that nucleation of α grains takes place at β–β grain boundaries and significant branching takes place after initial growth of α grains along β–β grain boundaries. Some branches grow inside the β grain interior. The branching behavior is shown to interact with β–β grain boundaries, leading to a zig-zag morphology. The presented 3-D analysis of α grains and their influence on β–β grain boundaries clearly show that 2-D observations of the microstructural morphologies are not sufficient to adequately represent the transformation characteristics. DEWEY : 669 ISSN : 1359-6454 En ligne : http://www.sciencedirect.com/science/article/pii/S1359645409008726

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