The deformation of Gum Metal through in situ compression of nanopillars / E.A. Withey in Acta materialia, Vol. 58 N° 7 (Avril 2010)  

Public ISBD [article]  inActa materialia > Vol. 58 N° 7 (Avril 2010) . - pp. 2652–2665 Titre : The deformation of Gum Metal through in situ compression of nanopillars Type de document : texte imprimé Auteurs : E.A. Withey, Auteur ; A.M. Minor, Auteur ; D. C. Chrzan, Auteur Année de publication : 2011 Article en page(s) : pp. 2652–2665 Note générale : Métallurgie Langues : Anglais (eng) Mots-clés : Compression test Titanium TEM Gum Metal Résumé : The name “Gum Metal” has been given to a set of β-Ti alloys that achieve exceptional elastic elongation and, with appropriate preparation, appear to deform by a dislocation-free mechanism triggered by elastic instability at the limit of strength. We have studied the compressive deformation of these materials with in situ nanocompression in a quantitative stage in a transmission electron microscope. The samples studied are cylindrical nanopillars 80–250 nm in diameter. The deformation pattern is monitored in real time using bright-field microscopy, dark-field microscopy or electron diffraction. Interesting results include the following: (i) nanopillars approach, and in several examples appear to reach, ideal strength; (ii) in contrast to conventional crystalline materials, there is no substantial “size effect” in pillar strength; (iii) the deformation mode is fine-scale with respect to the sample dimension, even in pillars of 100 nm size; (iv) shear bands (“giant faults”) do form in some tests, but only after yield and plastic deformation; and (v) a martensitic transformation to the base-centered orthorhombic α′′ phase is sometimes observed, but is an incidental feature of the deformation rather than a significant cause of it. DEWEY : 669 ISSN : 1359-6454 En ligne : http://www.sciencedirect.com/science/article/pii/S1359645409009100 [article] The deformation of Gum Metal through in situ compression of nanopillars [texte imprimé] / E.A. Withey, Auteur ; A.M. Minor, Auteur ; D. C. Chrzan, Auteur . - 2011 . - pp. 2652–2665. Métallurgie Langues : Anglais (eng) in Acta materialia > Vol. 58 N° 7 (Avril 2010) . - pp. 2652–2665 Mots-clés : Compression test Titanium TEM Gum Metal Résumé : The name “Gum Metal” has been given to a set of β-Ti alloys that achieve exceptional elastic elongation and, with appropriate preparation, appear to deform by a dislocation-free mechanism triggered by elastic instability at the limit of strength. We have studied the compressive deformation of these materials with in situ nanocompression in a quantitative stage in a transmission electron microscope. The samples studied are cylindrical nanopillars 80–250 nm in diameter. The deformation pattern is monitored in real time using bright-field microscopy, dark-field microscopy or electron diffraction. Interesting results include the following: (i) nanopillars approach, and in several examples appear to reach, ideal strength; (ii) in contrast to conventional crystalline materials, there is no substantial “size effect” in pillar strength; (iii) the deformation mode is fine-scale with respect to the sample dimension, even in pillars of 100 nm size; (iv) shear bands (“giant faults”) do form in some tests, but only after yield and plastic deformation; and (v) a martensitic transformation to the base-centered orthorhombic α′′ phase is sometimes observed, but is an incidental feature of the deformation rather than a significant cause of it. DEWEY : 669 ISSN : 1359-6454 En ligne : http://www.sciencedirect.com/science/article/pii/S1359645409009100

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