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Kinetic and thermodynamic investigation of lipase - catalyzed hydrolysis of (R,S) - 3 - phenylbutyl azolides

Jin-Ru Chen, Auteur ; Chia-Ching Wu, Auteur ; Pei-Yun Wang, Auteur |

Dans Industrial & engineering chemistry research (Vol. 51 N° 9, Mars 2012)

Water-saturated cydohexane at 25 °C is selected as the best reaction condition for Novozym 435-catalyzed hydrolytic resolution of (R,S)-3-phenylbutyl 4-methylpyazolide (1). The kinetic constants and enantiomeric ratio of 36 are then estimated fr[...]

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