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Application of mechanochemical pretreatment prior to aqueous extraction of eleutheroside B from eleutherococcus senticosus / Liji Jin in Industrial & engineering chemistry research, Vol. 51 N° 32 (Août 2012) 

Public ISBD [article]  in Industrial & engineering chemistry research > Vol. 51 N° 32 (Août 2012) . - pp. 10695-10701 Titre : Application of mechanochemical pretreatment prior to aqueous extraction of eleutheroside B from eleutherococcus senticosus Type de document : texte imprimé Auteurs : Liji Jin, Auteur ; Huaqiang Li, Auteur ; Feifei Wu, Auteur Année de publication : 2012 Article en page(s) : pp. 10695-10701 Note générale : Industrial chemistry Langues : Anglais (eng) Mots-clés : Pretreatment Résumé : A mechanochemical pretreatment was used prior to aqueous extraction of eleutheroside B from Eleutherococcus senticosus. The effects of the mechanochemical assisted extraction parameters hydroxypropyl-β-cyclodextrin (HP-β-CD) content, particle size, and circulating water temperature on the extraction yield of eleutheroside B were investigated. The mechanochemical assisted extraction process was optimized based on an orthogonal experimental design. The optimum process conditions were a HP-β-CD content of 23% (w/w), a particle size of D95 ≤ 44 μm and circulating water temperature of 40 °C. The mechanochemical assisted extraction process produced a higher eleutheroside B extraction yield, using a shorter extraction time and a greatly simplified process compared with traditional heat-reflux extraction, which makes mechanochemical assisted extraction a potential tool for eleutheroside B extraction from Eleutherococcus senticosus. Moreover, this technique used water as the solvent, making mechanochemical assisted extraction a less expensive and eco-friendly technique compared with traditional heat-reflux extraction. ISSN : 0888-5885 En ligne : http://cat.inist.fr/?aModele=afficheN&cpsidt=26259773 [article] Application of mechanochemical pretreatment prior to aqueous extraction of eleutheroside B from eleutherococcus senticosus [texte imprimé] / Liji Jin, Auteur ; Huaqiang Li, Auteur ; Feifei Wu, Auteur . - 2012 . - pp. 10695-10701. Industrial chemistry Langues : Anglais (eng) in Industrial & engineering chemistry research > Vol. 51 N° 32 (Août 2012) . - pp. 10695-10701 Mots-clés : Pretreatment Résumé : A mechanochemical pretreatment was used prior to aqueous extraction of eleutheroside B from Eleutherococcus senticosus. The effects of the mechanochemical assisted extraction parameters hydroxypropyl-β-cyclodextrin (HP-β-CD) content, particle size, and circulating water temperature on the extraction yield of eleutheroside B were investigated. The mechanochemical assisted extraction process was optimized based on an orthogonal experimental design. The optimum process conditions were a HP-β-CD content of 23% (w/w), a particle size of D95 ≤ 44 μm and circulating water temperature of 40 °C. The mechanochemical assisted extraction process produced a higher eleutheroside B extraction yield, using a shorter extraction time and a greatly simplified process compared with traditional heat-reflux extraction, which makes mechanochemical assisted extraction a potential tool for eleutheroside B extraction from Eleutherococcus senticosus. Moreover, this technique used water as the solvent, making mechanochemical assisted extraction a less expensive and eco-friendly technique compared with traditional heat-reflux extraction. ISSN : 0888-5885 En ligne : http://cat.inist.fr/?aModele=afficheN&cpsidt=26259773