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Integration of microreactors with spectroscopic detection for online reaction monitoring and catalyst characterization / Jun Yue in Industrial & engineering chemistry research, Vol. 51 N° 45 (Novembre 2012) 

Public ISBD [article]  in Industrial & engineering chemistry research > Vol. 51 N° 45 (Novembre 2012) . - pp 14583–14609 Titre : Integration of microreactors with spectroscopic detection for online reaction monitoring and catalyst characterization Type de document : texte imprimé Auteurs : Jun Yue, Auteur ; Jaap C. Schouten, Auteur ; T. Alexander Nijhuis, Auteur Année de publication : 2013 Article en page(s) : pp 14583–14609 Note générale : Industrial chemistry Langues : Anglais (eng) Mots-clés : Microreactors  Catalyst Résumé : Microreactor technology has gained significant popularity in the chemical and process industry in the past decade. The development of microreactors either as innovative production units for chemical synthesis or as promising laboratory tools for reaction and kinetic studies relies highly on the capability of performing online analyses, which opens great opportunities for the integration of spectroscopic detection techniques. This paper gives an overview of the state-of-the-art in the combination of microreactors with spectroscopic analyses for online reaction monitoring and catalyst characterization. In this upcoming field, many studies have been carried out combining fluorescence, ultraviolet–visible, infrared, Raman, X-ray, and nuclear magnetic resonance spectroscopy. Current research progress is reviewed, with emphasis on the existing integration schemes and selected application examples that demonstrate the potential of online spectroscopic detection for rapid microreactor process analysis and optimization. An outlook on the future development in this area is also presented. ISSN : 0888-5885 En ligne : http://pubs.acs.org/doi/abs/10.1021/ie301258j [article] Integration of microreactors with spectroscopic detection for online reaction monitoring and catalyst characterization [texte imprimé] / Jun Yue, Auteur ; Jaap C. Schouten, Auteur ; T. Alexander Nijhuis, Auteur . - 2013 . - pp 14583–14609. Industrial chemistry Langues : Anglais (eng) in Industrial & engineering chemistry research > Vol. 51 N° 45 (Novembre 2012) . - pp 14583–14609 Mots-clés : Microreactors  Catalyst Résumé : Microreactor technology has gained significant popularity in the chemical and process industry in the past decade. The development of microreactors either as innovative production units for chemical synthesis or as promising laboratory tools for reaction and kinetic studies relies highly on the capability of performing online analyses, which opens great opportunities for the integration of spectroscopic detection techniques. This paper gives an overview of the state-of-the-art in the combination of microreactors with spectroscopic analyses for online reaction monitoring and catalyst characterization. In this upcoming field, many studies have been carried out combining fluorescence, ultraviolet–visible, infrared, Raman, X-ray, and nuclear magnetic resonance spectroscopy. Current research progress is reviewed, with emphasis on the existing integration schemes and selected application examples that demonstrate the potential of online spectroscopic detection for rapid microreactor process analysis and optimization. An outlook on the future development in this area is also presented. ISSN : 0888-5885 En ligne : http://pubs.acs.org/doi/abs/10.1021/ie301258j